dor_id: 4132949

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650.#.4.x: Físico Matemáticas y Ciencias de la Tierra

336.#.#.b: article

336.#.#.3: Artículo de Investigación

336.#.#.a: Artículo

351.#.#.6: http://revistagi.geofisica.unam.mx/index.php/RGI

351.#.#.b: Geofísica Internacional

351.#.#.a: Artículos

harvesting_group: RevistasUNAM

270.1.#.p: Revistas UNAM. Dirección General de Publicaciones y Fomento Editorial, UNAM en revistas@unam.mx

590.#.#.c: Open Journal Systems (OJS)

270.#.#.d: MX

270.1.#.d: México

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883.#.#.q: Dirección General de Publicaciones y Fomento Editorial

850.#.#.a: Universidad Nacional Autónoma de México

856.4.0.u: http://revistagi.geofisica.unam.mx/index.php/RGI/article/view/403/416

100.1.#.a: Alva-valdivia, Luis M.; Rivas-sánchez, María De La Luz; Arenas-alatorre, Jesús; Goguitchaishvili, Avto; Ferreira Lopes, Omar

524.#.#.a: Alva-valdivia, Luis M., et al. (2013). Microscopy and rock magnetism of fine grain-size titanomagnetite from the Jacupiranga Alkaline Complex, Brazil: unearthing Ti-magnesioferrite nanoparticles. Geofísica Internacional; Vol. 52 Núm. 2: Abril 1, 2013; 93-110. Recuperado de https://repositorio.unam.mx/contenidos/4132949

245.1.0.a: Microscopy and rock magnetism of fine grain-size titanomagnetite from the Jacupiranga Alkaline Complex, Brazil: unearthing Ti-magnesioferrite nanoparticles

502.#.#.c: Universidad Nacional Autónoma de México

561.1.#.a: Instituto de Geofísica, UNAM

264.#.0.c: 2013

264.#.1.c: 2013-04-01

653.#.#.a: nanopartículas de titanomagnesioferrita; propiedades magnéticas; mineralogía; efecto del tamaño de grano; complejo alcalino Jacupiranga; Brasil; TMf nanoparticles; magnetic properties; mineralogy; grain size effect; Jacupiranga Alkaline Complex; Brazil

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884.#.#.k: http://revistagi.geofisica.unam.mx/index.php/RGI/article/view/403

001.#.#.#: 063.oai:revistagi.geofisica.unam.mx:article/403

041.#.7.h: spa

520.3.#.a: Very fine samples from the mineralized zones of the Jacupiranga complex at the Cajatí mine were selected for crystallographic identification of Ti-magnesioferrite (TMf) nanostructures embedded in titanomagnetite (TM) using high-resolution transmission electron microscopy (TEM). A magnetic concentrate obtained of pyroxenite samples (sites 4 to 7) was reduced and divided into fractions of distinct range sizes: 26±2 µm, 19±1 µm, 13±1 µm, 9±1 µm, 6±1 µm and 6–0.1 µm. The mineralized samples of carbonatite and pyroxenitewerecharacterized by X-ray diffraction, transmitted and reflected light microscope, and scanning electron microscope with multielemental analysis. The finest magnetic concentrate sample (MC6) was analyzed under high-resolution transmitted electron microscopy (TEM) and high angleannulardarkfield and Ramanspectroscopy. Magnetic properties were measured for the distinct granulometric fractions, showing drastic changes when grain sizes go beyond the frontier from micro to nanometer sizes. Frequency-dependent magnetic susceptibility percentage (χfd%) report higher values (10.2%) for the finer fractions (6±1 µm and 6–0.1 µm) attributed to dominant fractions of superparamagnetic particles. Nanometer and < 6 µm grain size TMf in TM particles require a magnetic field up to 249 mT to reach saturation during the isothermal remanent magnetization experiment. Coercivity and remanent magnetization of these samples increase when the particle size decreases, probably due to parallel coupling effects. Magnetic susceptibility versus temperature experiments were conducted two times on the same (< 35 nm) sample, showing that the repetition during the second heating is probably due to the formation of new TMf nanoparticles and growth of those already present during the first heating process.doi: https://doi.org/10.1016/S0016-7169(13)71465-X

773.1.#.t: Geofísica Internacional; Vol. 52 Núm. 2: Abril 1, 2013; 93-110

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300.#.#.a: Páginas: 93-110

264.#.1.b: Instituto de Geofísica, UNAM

doi: https://doi.org/10.1016/S0016-7169(13)71465-X

handle: 00f7bc08ea4a05fc

harvesting_date: 2023-06-20 16:00:00.0

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file_creation_date: 2013-03-21 19:41:25.0

file_modification_date: 2022-07-05 14:37:08.0

file_creator: Alva-Valdivia L.M.

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245.1.0.b: Microscopy and rock magnetism of fine grain-size titanomagnetite from the Jacupiranga Alkaline Complex, Brazil: unearthing Ti-magnesioferrite nanoparticles

last_modified: 2023-06-20 16:00:00

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Artículo

Microscopy and rock magnetism of fine grain-size titanomagnetite from the Jacupiranga Alkaline Complex, Brazil: unearthing Ti-magnesioferrite nanoparticles

Alva-valdivia, Luis M.; Rivas-sánchez, María De La Luz; Arenas-alatorre, Jesús; Goguitchaishvili, Avto; Ferreira Lopes, Omar

Instituto de Geofísica, UNAM, publicado en Geofísica Internacional, y cosechado de Revistas UNAM

Licencia de uso

Procedencia del contenido

Entidad o dependencia
Instituto de Geofísica, UNAM
Revista
Repositorio
Contacto
Revistas UNAM. Dirección General de Publicaciones y Fomento Editorial, UNAM en revistas@unam.mx

Cita

Alva-valdivia, Luis M., et al. (2013). Microscopy and rock magnetism of fine grain-size titanomagnetite from the Jacupiranga Alkaline Complex, Brazil: unearthing Ti-magnesioferrite nanoparticles. Geofísica Internacional; Vol. 52 Núm. 2: Abril 1, 2013; 93-110. Recuperado de https://repositorio.unam.mx/contenidos/4132949

Descripción del recurso

Autor(es)
Alva-valdivia, Luis M.; Rivas-sánchez, María De La Luz; Arenas-alatorre, Jesús; Goguitchaishvili, Avto; Ferreira Lopes, Omar
Tipo
Artículo de Investigación
Área del conocimiento
Físico Matemáticas y Ciencias de la Tierra
Título
Microscopy and rock magnetism of fine grain-size titanomagnetite from the Jacupiranga Alkaline Complex, Brazil: unearthing Ti-magnesioferrite nanoparticles
Fecha
2013-04-01
Resumen
Very fine samples from the mineralized zones of the Jacupiranga complex at the Cajatí mine were selected for crystallographic identification of Ti-magnesioferrite (TMf) nanostructures embedded in titanomagnetite (TM) using high-resolution transmission electron microscopy (TEM). A magnetic concentrate obtained of pyroxenite samples (sites 4 to 7) was reduced and divided into fractions of distinct range sizes: 26±2 µm, 19±1 µm, 13±1 µm, 9±1 µm, 6±1 µm and 6–0.1 µm. The mineralized samples of carbonatite and pyroxenitewerecharacterized by X-ray diffraction, transmitted and reflected light microscope, and scanning electron microscope with multielemental analysis. The finest magnetic concentrate sample (MC6) was analyzed under high-resolution transmitted electron microscopy (TEM) and high angleannulardarkfield and Ramanspectroscopy. Magnetic properties were measured for the distinct granulometric fractions, showing drastic changes when grain sizes go beyond the frontier from micro to nanometer sizes. Frequency-dependent magnetic susceptibility percentage (χfd%) report higher values (10.2%) for the finer fractions (6±1 µm and 6–0.1 µm) attributed to dominant fractions of superparamagnetic particles. Nanometer and < 6 µm grain size TMf in TM particles require a magnetic field up to 249 mT to reach saturation during the isothermal remanent magnetization experiment. Coercivity and remanent magnetization of these samples increase when the particle size decreases, probably due to parallel coupling effects. Magnetic susceptibility versus temperature experiments were conducted two times on the same (< 35 nm) sample, showing that the repetition during the second heating is probably due to the formation of new TMf nanoparticles and growth of those already present during the first heating process.doi: https://doi.org/10.1016/S0016-7169(13)71465-X
Tema
nanopartículas de titanomagnesioferrita; propiedades magnéticas; mineralogía; efecto del tamaño de grano; complejo alcalino Jacupiranga; Brasil; TMf nanoparticles; magnetic properties; mineralogy; grain size effect; Jacupiranga Alkaline Complex; Brazil
Idioma
spa
ISSN
ISSN-L: 2954-436X; ISSN impreso: 0016-7169

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