dor_id: 4129573

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351.#.#.b: Journal of Applied Research and Technology

351.#.#.a: Artículos

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856.4.0.u: https://jart.icat.unam.mx/index.php/jart/article/view/1324/921

100.1.#.a: Setianingsih, Tutik; Susilo, Bambang; Mutrofin, Siti; Ismuyanto, Bambang; Endaryana, Andreas Novan; Yoniansyah, Yoandra Nadya

524.#.#.a: Setianingsih, Tutik, et al. (2022). Influence of sequential pyrolisis methods on the properties of the carbon nanostructure (CNS) from sugarcane leaf biomass. Journal of Applied Research and Technology; Vol. 20 Núm. 4, 2022; 460-471. Recuperado de https://repositorio.unam.mx/contenidos/4129573

245.1.0.a: Influence of sequential pyrolisis methods on the properties of the carbon nanostructure (CNS) from sugarcane leaf biomass

502.#.#.c: Universidad Nacional Autónoma de México

561.1.#.a: Instituto de Ciencias Aplicadas y Tecnología, UNAM

264.#.0.c: 2022

264.#.1.c: 2022-08-31

653.#.#.a: sequential pyrolisis method; correlation of properties; carbon nano structure

506.1.#.a: La titularidad de los derechos patrimoniales de esta obra pertenece a las instituciones editoras. Su uso se rige por una licencia Creative Commons BY-NC-SA 4.0 Internacional, https://creativecommons.org/licenses/by-nc-sa/4.0/legalcode.es, para un uso diferente consultar al responsable jurídico del repositorio por medio del correo electrónico gabriel.ascanio@icat.unam.mx

884.#.#.k: https://jart.icat.unam.mx/index.php/jart/article/view/1324

001.#.#.#: 074.oai:ojs2.localhost:article/1324

041.#.7.h: eng

520.3.#.a: Plant biomass is a potential lignocellulose material for synthesis of carbon nano structure. Its characteristics as adsorbent and its size particle make it good additive for liquid fertilizer. In this research, we study influence of sequential different pressure pyrolysis methods (hydrothermal–microwave method and reflux–microwave method) toward characteristics of carbon nanostructure from sugarcane leaf biomass. Each reflux and hydrothermal method was adjusted at 200oC, then followed by microwave at 800W. Characterization showed that the hydrothermal - microwave method using X-ray diffraction indicates diffractogram patterns of both carbon nanostructure and cellulose. SEM micrographs show sphere and block shapes. FTIR spectra indicates different concentration of oxy surface functional groups. UV spectra of the dispersed product in water indicates existence of aromatics C=C groups. The hydrothermal - microwave method resulted the product inwhich lower crystalinity index of cellulose, smaller particles, lower concentration of oxy surface groups than the reflux - microwave one. Correlation of chemical properties (aromaticity and fraction of polar groups) was more linier than of physical - chemical properties (indexe of cellulose crystalinity and fraction of polar groups). The stability of colloid was indicated by dispersing technique in order of sonication < blending < blending - sonication.

773.1.#.t: Journal of Applied Research and Technology; Vol. 20 Núm. 4 (2022); 460-471

773.1.#.o: https://jart.icat.unam.mx/index.php/jart

022.#.#.a: ISSN electrónico: 2448-6736; ISSN: 1665-6423

310.#.#.a: Bimestral

300.#.#.a: Páginas: 460-471

264.#.1.b: Instituto de Ciencias Aplicadas y Tecnología, UNAM

doi: https://doi.org/10.22201/icat.24486736e.2022.20.4.1324

harvesting_date: 2023-11-08 13:10:00.0

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Artículo

Influence of sequential pyrolisis methods on the properties of the carbon nanostructure (CNS) from sugarcane leaf biomass

Setianingsih, Tutik; Susilo, Bambang; Mutrofin, Siti; Ismuyanto, Bambang; Endaryana, Andreas Novan; Yoniansyah, Yoandra Nadya

Instituto de Ciencias Aplicadas y Tecnología, UNAM, publicado en Journal of Applied Research and Technology, y cosechado de Revistas UNAM

Licencia de uso

Procedencia del contenido

Cita

Setianingsih, Tutik, et al. (2022). Influence of sequential pyrolisis methods on the properties of the carbon nanostructure (CNS) from sugarcane leaf biomass. Journal of Applied Research and Technology; Vol. 20 Núm. 4, 2022; 460-471. Recuperado de https://repositorio.unam.mx/contenidos/4129573

Descripción del recurso

Autor(es)
Setianingsih, Tutik; Susilo, Bambang; Mutrofin, Siti; Ismuyanto, Bambang; Endaryana, Andreas Novan; Yoniansyah, Yoandra Nadya
Tipo
Artículo de Investigación
Área del conocimiento
Ingenierías
Título
Influence of sequential pyrolisis methods on the properties of the carbon nanostructure (CNS) from sugarcane leaf biomass
Fecha
2022-08-31
Resumen
Plant biomass is a potential lignocellulose material for synthesis of carbon nano structure. Its characteristics as adsorbent and its size particle make it good additive for liquid fertilizer. In this research, we study influence of sequential different pressure pyrolysis methods (hydrothermal–microwave method and reflux–microwave method) toward characteristics of carbon nanostructure from sugarcane leaf biomass. Each reflux and hydrothermal method was adjusted at 200oC, then followed by microwave at 800W. Characterization showed that the hydrothermal - microwave method using X-ray diffraction indicates diffractogram patterns of both carbon nanostructure and cellulose. SEM micrographs show sphere and block shapes. FTIR spectra indicates different concentration of oxy surface functional groups. UV spectra of the dispersed product in water indicates existence of aromatics C=C groups. The hydrothermal - microwave method resulted the product inwhich lower crystalinity index of cellulose, smaller particles, lower concentration of oxy surface groups than the reflux - microwave one. Correlation of chemical properties (aromaticity and fraction of polar groups) was more linier than of physical - chemical properties (indexe of cellulose crystalinity and fraction of polar groups). The stability of colloid was indicated by dispersing technique in order of sonication < blending < blending - sonication.
Tema
sequential pyrolisis method; correlation of properties; carbon nano structure
Idioma
eng
ISSN
ISSN electrónico: 2448-6736; ISSN: 1665-6423

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