dor_id: 22989

506.#.#.a: Público

590.#.#.d: Los artículos enviados a la "Revista Internacional de Contaminación Ambiental" se juzgan por medio de un proceso de revisión por pares

510.0.#.a: Consejo Nacional de Ciencia y Tecnología (CONACyT); Sistema Regional de Información en Línea para Revistas Científicas de América Latina, el Caribe, España y Portugal (Latindex); Scientific Electronic Library Online (SciELO); SCOPUS, Web Of Science (WoS); Aquatic Sciences and Fisheries Abstracts, Cab Abstracts, Cab Health, Chemical Abstracts, Elsevier Biobase, Elsevier Geo Abstracts, Periódica, Pollution Abstracts, SCOPUS, Water Resources Abstracts

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650.#.4.x: Biología y Química

336.#.#.b: article

336.#.#.3: Artículo de Investigación

336.#.#.a: Artículo

351.#.#.6: https://www.revistascca.unam.mx/rica/index.php/rica/index

351.#.#.b: Revista Internacional de Contaminación Ambiental

351.#.#.a: Artículos

harvesting_group: RevistasUNAM

270.1.#.p: Revistas UNAM. Dirección General de Publicaciones y Fomento Editorial, UNAM en revistas@unam.mx

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270.#.#.d: MX

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590.#.#.a: Coordinación de Difusión Cultural

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850.#.#.a: Universidad Nacional Autónoma de México

856.4.0.u: https://www.revistascca.unam.mx/rica/index.php/rica/article/view/RICA.2018.34.02.15/46763

100.1.#.a: Sánchez Uría, José Enrique; del Castillo Busto, Estela

524.#.#.a: Sánchez Uría, José Enrique, et al. (2018). ANALYTICAL PERFORMANCE OF MICROWAVE-ASSISTED SOLVENT EXTRACTION (MASE) FOR THE ROUTINE DETERMINATION OF PAHs IN POLLUTED SOILS BY GAS CHROMATOGRAPHIC-MASS SPECTROMETRY (GC-MS). Revista Internacional de Contaminación Ambiental; Vol. 34 Núm. 2, 2018; 355-366. Recuperado de https://repositorio.unam.mx/contenidos/22989

245.1.0.a: ANALYTICAL PERFORMANCE OF MICROWAVE-ASSISTED SOLVENT EXTRACTION (MASE) FOR THE ROUTINE DETERMINATION OF PAHs IN POLLUTED SOILS BY GAS CHROMATOGRAPHIC-MASS SPECTROMETRY (GC-MS)

502.#.#.c: Universidad Nacional Autónoma de México

561.1.#.a: Instituto de Ciencias de la Atmósfera y Cambio Climático, UNAM

264.#.0.c: 2018

264.#.1.c: 2018-04-30

653.#.#.a: pollutants; analysis; method; solid; samples; Polycyclic Aromatic Hydrocarbons; soils; Gas Chromatography; Mass Spectrometry; Microwave Assisted Solvent Extraction

506.1.#.a: La titularidad de los derechos patrimoniales de esta obra pertenece a las instituciones editoras. Su uso se rige por una licencia Creative Commons BY-NC 4.0 Internacional, https://creativecommons.org/licenses/by-nc/4.0/legalcode.es, para un uso diferente consultar al responsable jurídico del repositorio por medio del correo electrónico claudio.amescua@atmosfera.unam.mx

884.#.#.k: https://www.revistascca.unam.mx/rica/index.php/rica/article/view/RICA.2018.34.02.15

001.#.#.#: 105.oai:ojs.pkp.sfu.ca:article/52295

041.#.7.h: spa

520.3.#.a: The extraction of PAHs from polluted soil samples using Microwave Assited Solvent Extraction (MASE) with subsequent determination by Gas Chromatography-Mass Spectrometry (GC-MS) was investigated. Optimum conditions for the extraction are established and after the cleansing of extracts, those pollutants were quantified by GC-MS. Detection limits for the 16 US-EPA members of the family, analysis time, precision and linear range of the analysis have been also established. The proposed extraction methodology was compared with the most conventional Soxhlet extraction technique, and validated by applying the MASE to a reference soil sample. Good recoveries for the majority of PAHs (when calibrations were carried out by using internal standards), significant shortening time of analysis and reduction of volume of solvent used were observed. Thus, the MASE sample preparation methodology constitutes a very good alternative to extraction of PAHs from soil samples before the final determination by GC-MS.

773.1.#.t: Revista Internacional de Contaminación Ambiental; Vol. 34 Núm. 2 (2018); 355-366

773.1.#.o: https://www.revistascca.unam.mx/rica/index.php/rica/index

022.#.#.a: ISSN impreso: 0188-4999

310.#.#.a: Trimestral

300.#.#.a: Páginas: 355-366

264.#.1.b: Instituto de Ciencias de la Atmósfera y Cambio Climático, UNAM

doi: https://doi.org/10.20937/RICA.2018.34.02.15

harvesting_date: 2023-11-08 13:10:00.0

856.#.0.q: application/pdf

245.1.0.b: ANALYTICAL PERFORMANCE OF MICROWAVE ASSISTED SOLVENT EXTRACTION (MASE) FOR ROUTINE DETERMINATION OF PAHs IN POLLUTED SOILS BY GAS CHROMATOGRAPHIC-MASS SPECTROMETRY (GC-MS).

last_modified: 2024-03-19 14:00:00

license_url: https://creativecommons.org/licenses/by-nc/4.0/legalcode.es

license_type: by-nc

_deleted_conflicts: 2-f5eb2300c6541e0f7c30a62544fd436f

No entro en nada

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Artículo

ANALYTICAL PERFORMANCE OF MICROWAVE-ASSISTED SOLVENT EXTRACTION (MASE) FOR THE ROUTINE DETERMINATION OF PAHs IN POLLUTED SOILS BY GAS CHROMATOGRAPHIC-MASS SPECTROMETRY (GC-MS)

Sánchez Uría, José Enrique; del Castillo Busto, Estela

Instituto de Ciencias de la Atmósfera y Cambio Climático, UNAM, publicado en Revista Internacional de Contaminación Ambiental, y cosechado de Revistas UNAM

Licencia de uso

Procedencia del contenido

Cita

Sánchez Uría, José Enrique, et al. (2018). ANALYTICAL PERFORMANCE OF MICROWAVE-ASSISTED SOLVENT EXTRACTION (MASE) FOR THE ROUTINE DETERMINATION OF PAHs IN POLLUTED SOILS BY GAS CHROMATOGRAPHIC-MASS SPECTROMETRY (GC-MS). Revista Internacional de Contaminación Ambiental; Vol. 34 Núm. 2, 2018; 355-366. Recuperado de https://repositorio.unam.mx/contenidos/22989

Descripción del recurso

Autor(es)
Sánchez Uría, José Enrique; del Castillo Busto, Estela
Tipo
Artículo de Investigación
Área del conocimiento
Biología y Química
Título
ANALYTICAL PERFORMANCE OF MICROWAVE-ASSISTED SOLVENT EXTRACTION (MASE) FOR THE ROUTINE DETERMINATION OF PAHs IN POLLUTED SOILS BY GAS CHROMATOGRAPHIC-MASS SPECTROMETRY (GC-MS)
Fecha
2018-04-30
Resumen
The extraction of PAHs from polluted soil samples using Microwave Assited Solvent Extraction (MASE) with subsequent determination by Gas Chromatography-Mass Spectrometry (GC-MS) was investigated. Optimum conditions for the extraction are established and after the cleansing of extracts, those pollutants were quantified by GC-MS. Detection limits for the 16 US-EPA members of the family, analysis time, precision and linear range of the analysis have been also established. The proposed extraction methodology was compared with the most conventional Soxhlet extraction technique, and validated by applying the MASE to a reference soil sample. Good recoveries for the majority of PAHs (when calibrations were carried out by using internal standards), significant shortening time of analysis and reduction of volume of solvent used were observed. Thus, the MASE sample preparation methodology constitutes a very good alternative to extraction of PAHs from soil samples before the final determination by GC-MS.
Tema
pollutants; analysis; method; solid; samples; Polycyclic Aromatic Hydrocarbons; soils; Gas Chromatography; Mass Spectrometry; Microwave Assisted Solvent Extraction
Idioma
spa
ISSN
ISSN impreso: 0188-4999

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